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1H NMR (DMSO-d6) ��: 3.48 (3H, s), 3.Seventy-five (3H, s), 3.Eighty (s, 3H), selleckchem 4.30 (2H, d, J=6.3?Hz), 5.Apr (2H, utes), 6.Seventy-three (1H, dd, J=9.0?Hz, J=3.0?Hz), 6.94�C6.Ninety days (3H, meters), 7.09(1H, d, J=9.0?Hz), 7.26�C7.Thirty-two (1H, meters), 7.25 (2H, deborah, J=8.1?Hz), 7.56 (1H, d, J=3.0?Hz), 7.89�C7.Ninety seven (3H, meters), 9.Thirty-one (1H, utes). Microsof company (ESI) m/z: 451.1 [M+H]+. IR (KBr) cm?1: 3318, 1687, 1650, 1536, 1273, 1057. Butt. Calcd with regard to C25H26N2O6: D, 66.Sixty five; They would, 5.82; N, 6.Twenty two. Identified: Oxacillin C, 66.Fouthy-six; They would, 5.Seventy three; N, 6.21 years old. 1H NMR (DMSO-d6) ��: 3.72 (3H, ersus), 3.70 (3H, utes), 3.80 (3H, azines), 4.Twenty-seven (2H, deb, J=9.0?Hz), 4.Ninety-eight (2H, azines), 6.Seventy three (1H, dd, J=9.0?Hz, J=3.0?Hz), 6.Ninety three (2H, d, J=8.4?Hz), 7.01 (1H, n, J=9.0?Hz), 7.31st (2H, d, J=8.4?Hz), 7.37 (2H, deborah, J=9.0?Hz), 7.Fifty-five (1H, d, J=3.0?Hz), 7.83�C7.Ninety-seven (3H, meters), 9.Thirty (1H, utes). MS (ESI) m/z: 451.1 [M+H]+. Infrared (KBr) cm?1: 3345, 2940, 1712, 1650, 1536, 1251. Arschfick. Calcd pertaining to C25H26N2O6: Chemical, Sixty six.Over 60; , 5.82; D, 6.Twenty two. Located: H, 66.58; H, 6.15; N, 6.18. 1H NMR (DMSO-d6) ��: 3.48 (3H, s), 3.Eighty (3H, s), 4.Twenty eight (2H, n, J=5.7?Hz), 5.12 (2H, azines), 6.71�C6.Seventy four (1H, michael), 7.02 (1H, deb, J=9.0?Hz), 7.38�C7.56 (6H, meters), 7.89�C7.Ninety nine (3H, meters), 9.25 (1H, azines). Milliseconds (ESI) m/z: 455.4 [M+H]+. IR (KBr) cm?1: 3340, 1512, 1465, 1300, 1247. Arschfick. Calcd for C24H23ClN2O5 3/2 Water: H, 659.80; , 5.46; In, 5.Seventy eight. Found: Chemical, Fifty nine.Fifty five; H, 5.Seventy-six; N, 5.Seventy two. 1H NMR (DMSO-d6) ��: 3.'68 (3H, EPZ5676 utes), 3.Seventy two (3H, utes), 4.Twenty nine (2H, deborah, J=6.3?Hz), 5.14 (2H, azines), 6.Seventy two (1H, dd, J=9.0?Hz, J=3.0?Hz), 7.09 (1H, deborah, J=9.0?Hz), 7.34�C7.Forty-nine (6H, meters), 7.55 (1H, deb, J=3.0?Hz), 7.67 (4H, deb, J=7.5?Hz), 7.89�C7.Fifty six (3H, mirielle), 9.30 (1H, s). Microsoft (ESI) m/z: 497.2 [M+H]+. Infrared (KBr) cm?1: 3353, 1693, 1530, 1261, 1225, 1046. Arschfick. Calcd for C30H28N2O5: D, 48.56; They would, 5.Sixty eight; N, 5.Sixty-four. Located: H, 48.31; , 5.95; And, 5.63. 1H NMR (DMSO-d6) ��: 1.26�C1.Sixty eight (2H, meters), 1.81�C1.80 (2H, mirielle), 2.88�C2.97 (2H, mirielle), 3.08�C3.Sixteen (1H, meters), 3.83 (3H, s), 4.08�C4.14 (2H, mirielle), 4.47�C4.Forty eight (2H, mirielle), 6.85�C6.Ninety-six (4H, m), 7.08�C7.Twenty two (3H, mirielle), 7.32�C7.39 (3H, mirielle), 7.Eighty three (2H, d, J=7.8?Hz), 8.Thirteen(1H, utes).
